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Adsorbents for the Motor Fuel HF Alkylation Process

The motor fuel HF alkylation process catalytically combines C3-C5 olefins with isobutane to produce motor fuel alkylate, which is ideal for producing reformulated gasoline. There are two major licensors of this technology. Both licensors require careful control of the moisture content of both the feed olefin and saturate streams in order to minimize acid consumption. UOP adsorbents, both molecular sieves and aluminas, are highly-efficient dehydration adsorbents in this application.

When the feeds are contaminated by high levels of other contaminants, such as oxygenates (MTBE raffinate) or nitriles (FCC product contaminants), it’s desirable to remove such contaminants so as to minimize acid consumption and by-product formation. The UOP Oxygenate Removal unit (ORU) and the UOP Nitrile Removal unit (NRU) employ molecular sieve adsorbents that are highly effective in the purification of olefin-containing streams.

Each of the products from the HF alkylation process – propane, butanes and alkylate – contain traces of HF, as well as combined fluorides. In order to meet LPG specifications (C3 and C4 fractions), refiners employ activated alumina adsorbents to catalyze decomposition of the combined fluorides at elevated temperatures followed by removal of the HF formed by this reaction. Some refiners also employ these adsorbents to reduce the fluoride content of the alkylate product. Temperatures of 350°F– 450°F are necessary to catalytically decompose the organic fluorides to HF and an olefin. The HF produced rapidly reacts with the high surface area, high porosity alumina to form aluminum fluoride, thereby removing fluorides from the hydrocarbon streams. You can look to UOP A-202HF and P-188 adsorbents as commercially proven, cost-effective solutions for this application.

UOP also offers a unique Recoverable Aluminum Fluoride (RALF) program for the recovery of the alumina product from spent material. All spent alumina needs to meet certain specifications (> 95% of the time) before the alumina can be reprocessed in this program. Once approved, for a nominal shipping charge, you will have a cost-effective source for reprocessing and reusing your spent alumina.

For more information on our HF alkylation adsorbent solutions, contact us using our information request form or contact your local sales office.

For more on related UOP technologies, click on the following links:
Light Olefin Conversion to Gasoline
Linear Alkylbenzene Production